Entry
Br2(eq.)
H2O (eq.)
m (Br2-H2O)/mg
T/℃
Yield/3a%b
Yield/4a%b
1
0.2
9.3
20
100
58
0
2
0.3
14
30
100
55
0
3
0.4
18.7
40
100
53
0
4
0.2
9.3
20
120
70
0
5
0.3
14
30
120
77
0
6
0.4
18.7
40
120
76
0
7
0.6
28
60
120
57
0
8
0.3
14
30
160
25
43
|
||||||
Entry |
Br2(eq.) |
H2O (eq.) |
m (Br2-H2O)/mg |
T/℃ |
Yield/3a%b |
Yield/4a%b |
1 |
0.2 |
9.3 |
20 |
100 |
58 |
0 |
2 |
0.3 |
14 |
30 |
100 |
55 |
0 |
3 |
0.4 |
18.7 |
40 |
100 |
53 |
0 |
4 |
0.2 |
9.3 |
20 |
120 |
70 |
0 |
5 |
0.3 |
14 |
30 |
120 |
77 |
0 |
6 |
0.4 |
18.7 |
40 |
120 |
76 |
0 |
7 |
0.6 |
28 |
60 |
120 |
57 |
0 |
8 |
0.3 |
14 |
30 |
160 |
25 |
43 |